Showing posts with label ambergris. Show all posts
Showing posts with label ambergris. Show all posts

Friday, June 07, 2013

Making Queen's Royal

I finally had time and material enough to try out Queen's Royal, the mystery recipe I talked about here.

Updated recipe
1 gramme each of brown ochre, rose-pink, red and black pigment. I used cosmetic pigment meant for soap making.
60 drops of Bergamot essential oil
30 drops of Lemon essential oil
10 drops of Lavender essential oil
10 drops of Caraway essential oil
6 drops of faux Ambergris oil
10 drops of Clove essential oil
6 drops of Rosemary essential oil
10 drops of Cinnamon essential oil


In the original recipe only the Bergamot and Lemon are stated to be essential oil, the rest are just oils. Essential oils are made by distillation, but you can also perfume oils by steeping the scent material in it for some time. 18th century recipes are notoriously unclear of what is used so even if the recipe might suggest that the two different kinds, that might not be the case. As essential oils are what is readily available if I used that. Essential oils are not particularly oily, so if using the other kind, the end result would be fatter. As for the pigments, Ican't be sure on the exact shades that were used in the 18th century. Black is, I suppose black, and the original Vermillion is a warm-toned red. Brown ochre is a warm-toned brown, but the rose-pink? I'm not sure. I used a fairly pale pink as that was what I found, but rose-pink could mean a pink more akin toward red.

I mixed the pigments and then I dripped in the essential oils before I mixed it very well. The end result was a rather stiff paste in dark brown with reddish hints. It first smelled very strongly of the Bergamot and Lemon, but after a while is smelled more spicy, with Cinnamon as the dominant smell. At first it was easy to spread out, but the essential oils evaporated quite quickly and the dried out pigment crumbled into powder when touched. I tried out the various thoughts and suggestion of the purpose of this scented mystery and here are the results. I've lumped similar suggestion together.

A scented powder to make into sachets? No. Scentwise it would work, but the very fine and very brown powder would eventually work itself out of a fabric sachet and discolour things around it. no sense in using pigment is something that you can't see.

A rouge for cheeks or for the nipples? For cheek rouge I would say a definite no- it is far too brown. As nipple rouge, though, I think it is plausible. It was very easy to spread out on skin and though it tingled slightly upon application due to the cinnamon, that feeling disappeared very quickly. I applied it thickly, medium thick and thinly on my arm and found that the two thicker layer started to shed pigment as soon as it dried out. There are nothing in this recipe that would help it adhere like Gum Arabic. The sheer application stayed on quite well, though. here.) So yes, I think this recipe may have been meant to tint nipples. However, the pigment rub off at the touch so even if it would show up if covered by a lightweight chemise, it would also discolour the fabric, so it would only be useful if the nipples were completely bare. The scent would work well here too, as it would drift up from the chest.
The pigment is clearly brown, but with a warm red tone on my arm so for the sake of science I did try it on a nipple as well. No, there are no pictures of that, you will just have to believe me. I can tell you that the result was a darker nipple that still looked fairly natural. I did some research in the habit of showing the breasts in the 17th and 18th century and though never common, it was fashionable from time to time and it was not completely uncommon on stage and masquerades. (A whole blog post dedicated to the subject can be found here.)

Tinted perfume meant for hair powder? As the end result is a brown pigment with a scent, this could work. In fact, the only thing against it, is the fact that all the other hair recipes in the book are all together and clearly stated to be just hair powders. There is also a recipe for dark brown hair powder, so why not put this together with that one?

To tint grey hair? Probably not as the preferred method to hide grey hair in the 18th century was to powder everything white. I did smear some in my hair though, and it did turn nicely brown, so it would work. It doesn't adhere well, though.


For tinting eyebrows or pubic hair? Plausible when it comes to tinting eyebrows. I used a stiff brush to paint my eyebrows and it worked remarkably well, making them dark, but not as harshly dark as a black tint. I was a bit worried that the scent would irritate my eyes, but there was no problems at all. I left it on for an hour or so and during that time the scent drifted around my face, but not very strongly. I have actually read modern perfume tips that you should perfume your eyebrows as perfume lasts longer on hair than skin. As for pubic hair, well... I did not try that- I hope you excuse me for not going all the way, but I don't think it would work anyway. It would just rub off on clothes, I think.

A repellant for lice? I can imagine that the scent could be thought to repel vermin, but the pigment would make everything it touched brown, so I don't think so.

Scented pastilles for burning? Possible. The pigment was easy to shape into pellets, they were almost impossible to handle when they were dry, due to teh fact there is no binding agent. They did burn, though, with an alarmingly huge flame. While it burned the only smell I got was smoke, but with the flame extinguished the smell of the essentials oil came through much stronger. So burn and smell-wise it worked. What talks against is is the lack of a binding agent. As they are now they would crumble into dust with a minimum of handling. However, as a powder it would probably work to trow it into a fire to scent a room. I have never heard of that method being employed in the 18th century, though. The biggest argument against it, is the use of pigment. Pigment was expensive and though one might want to colour something to make it pretty before use, the dark brown of this recipe isn't very pretty at all. So why use up a lot of expensive pigment just to burn it?

I didn't try the last suggestion, though:

To rub into a porous material to give scent and tint? That would work, I think, on wood or bone, but again, I would think it would discolour everything it would come into contact with, unless one sealed the pigment in some way. And would that not mean sealing off the scent as well?

As you can see, the result is inconclusive. There are a few things that it very probably wasn't used as and some that are possible. To my mind the most plausible uses are eyebrow or nipple tint as that seems to make the most use of both pigment and scent. What do you think? Or perhaps you have an idea that is much better that I haven't thought of? I promise, if I find out more, I will keep you updated. It was a lot of fun doing this experiment, though!

One thing I consider doing is to mix the same proportions of the esential oil together, adding a neutral oil to make a perfume oil. Though it wouldn't, strictly speaking, be an original perfume recipe, it would still be an 18th century perfume blend.

Tuesday, April 30, 2013

Cyprian powder


Lady at Toilette, Utrecht school, 17th century
Click on the link for a fun article on 17th century beauty.
Today I have a 17th century perfume recipe for you, taken from Polygraphice by William Salmon, published in 1685.

The recipe
To make Cyprian Powder.
Gather Musk moss of the Oak in December, January or Februarys wash it very clean in Rose-water, then dry it, steep it in Rose-water for two days, then dry it again, which do oftentimes: then bring it into fine Powder and fierce it: of which take one pound, Musk one ounce, Ambergrise half an ounce, Civet two drachms, yellow Sanders in powder two ounces, mix all well together in a marble mortar.

Another way to make the same.
Take of the aforesaid powder of Oak-moss one pound, Benjamin, Storax of each two ounces in fine Powder: Musk .Ambergrise and Civet of each three drachms, mix them well in a mortar.

 Breaking down the recipe
Oak moss Despite the name, this is really a lichen, Evernia prunastri, and has been used in perfumes since the Middle ages. The scent has been described as dry, woody, and smoky with a hint of tar. Used as fixatives in modern perfumes, or rather, a synthetic is, real oak moss is now forbidden, and is often used in men’s perfumes and in the perfume family that is called chypre.

Musk A common base notes in perfumery derived from glands from various animals. Today synthetic musk is almost exclusively used. Musk in large doses smells rather pungent, but diluted it is a warm, sweet and woody scent.

Ambergris A base notes in perfumery with a sweet, vanilla-ish scent with aquatic undertones. It comes from the intestines of sperm whales that habitually vomit out lumps of ambergris, which then age into scent maturity by the sea water. Though it is perfectly, even preferable, possible with ethically gathered ambergris, it is also very expensive and synthetics are almost always used today.

Civet Another animalistic base note, derived from the civet. It is similar to musk, but even more pungent concentrated and more sweet, smoky and sharp when diluted. Nowadays usually a synthetic.

Yellow sanders Wood from a tree, Zanthoxylum flavum. The scented and durable tree is on the brink of being endangered, unfortunately.

Other ingredients can be found at the ingredient list at the top of the page

My thoughts
I bought some oak moss last year and have wanted to try my hands at a Cyprian, or Cyprus powder for some time. It was a popular perfume in the 17th and 18th century as well as the 19th. In the 18th century it was popular to mix it into hair powder to scent it, but it can also be sewn into small sachets to be worn inside clothes or pockets. There are several recipes around and they are all rather alike. Unlike modern perfumes that consist of base, middle and top notes, this perfume is all base notes. Such notes are long-lasting and often quite heavy.  I’m going to make this recipe, as I have vegetal musk, civet and ambergris substitute that I want to try. It is a very easy recipe. Wash, dry, steep dry and pound. I have actually done the first steps. The oak moss is currently steeping and smells quite lovely of roses and rain wet forests.

Wednesday, April 24, 2013

Queen's Royal, a cosmetic mystery

Theophila Palmer Reading Clarissa by Joshua Reynolds, 1771
I have encountered a little mystery. At the very last page of Charles Lillie’s The British perfumer we find the following recipe, which completely stumps me. I have absolutely no idea what it is supposed to be used for. Lillie wrote his manuscript in the 1740’s though it wasn’t published until 1822. The publisher has kindly provided notes of enlightenment on several recipes, but not on this one.

The recipe
QUEEN'S ROYAL:
Take one ounce of brown ochre,
One ounce of vermillion,
One ounce of rose-pink,
One ounce of ivory-black,
 
Three ounces of essence of bergamot,
One and a half ounce of essence of lemon,
Half an ounce of oil of lavender.
Half an ounce of oil of carraways, A quarter of an ounce of oil of ambergris,
Half an ounce of oil of cloves,
A quarter of an ounce of oil of rosemary,
and Half an ounce of oil of cinnamon.
 
These are to be well mixed together; but care must previously be taken to reduce the first-mentioned ingredients into very fine powder.

My thoughts
The recipe is in two parts. In the first several, finely milled, pigments are mixed in brown, red, pink and black. The first three would make a reddish brown; the addition of black will make the colour darker and duller. Pigments were expensive so there must be a reason for them to be in there. They must be meant to give something colour.

The second part is purely scent. Bergamot and lemon essence with oils of lavender, caraway, ambergris, clove, rosemary and cinnamon. That’s a lot of scent and several of the oil is very strongly scented like cinnamon and clove. So this is clearly meant to smell. Mixing pigments and scent together would either give a scented pigment or a paste. It is a bit hard to say until you have tried as it depends on the ratio between powder and liquid. I lean on a paste, but I’m not sure. And what was it used for? I have a few ideas, but they are just theories.

A scented powder to make into sachets? I don’t think so. Too much valuable pigment to hide away. Had it was meant for that purpose, the scent would have been mixed with starch.

A rouge? I don’t think so either. With ¼ black pigment the shade would most likely to be too dark and unbecoming. Also, cinnamon and clove oils can sting and redden skin upon application and would be uncomfortable to have on your face.

Can in be a tinted perfume meant for hair powder? Might be, but in that case it needs to be mixed with hair powder. Now I know that 18th century recipes aren’t always constant, but the other scented powders in this book are placed together and they also have clear instruction of the ratio between scented powder and hair powder.

For tinting eyebrows? That doesn’t seem too unlikely, but why not say so? The colour could work for hair and to scent your eyebrows aren’t that far-flung, actually- I have encountered that notion elsewhere, though never in an 18th century context.

Then I got a suggestion from a friend, and, well, it doesn’t seem too unlikely. That would explain why it is tucked away at the last page and that it lacks any kind of direction. Could this be meant to rub into the hair of your nether region? It would tint it and scent it, and might that be something that would be considered attractive? I balked at the thought of cinnamon oil on those parts but I have been informed that today you can buy oils, often containing just cinnamon that are actually meant to be used down there for added stimulation. So can this be a more risqué cosmetics for ladies (and gentlemen) who dared? What do you think? Or perhaps you have an excellent idea of what this was really used for that I haven’t thought about. I would love to hear what you think!

Sunday, February 10, 2013

Honey water

 
Eliza Smith’s Compleat Housewife, or Accomplish’d Gentlewoman’s Companion,
 1727
After my post on hair powder I really had to look up the Honey water mentioned in the brown powder recipe. Curiously enough this perfume, despite the name, doesn’t contain any honey. It is also a long recipe; though I will try to break it down to make it easier to overview. 

The recipe
AQUA-MELLIS, OR THE KING'S HONEYWATER.

Take twenty-eight pounds of coriander seeds, ground small in the starch-mill; twenty-eight common bunches of sweet marjoram, in flower, dried and stripped from the twigs, one pound of calamus aromaticus, one pound of yellow saunders, and one pound of orange and lemon peel. Let the three last mentioned substances be separately beaten into gross powder.

Mix the above ingredients, and put them into a sixty-gallon copper-still, and add to them twenty gallons of proof spirits, and the same quantity of rain or spring water.Lute well all the junctures of the apparatus, and leave the ingredients in this state, without fire, for forty-eight hours. At the end of this time, begin to distil by a very gentle heat, lest the flowers and seeds, which are very light, should rise suddenly in the still-head, stop up the worm, and endanger the whole work.

Increase the fire after the first half hour, and keep it regular, thereafter, till the termination of the process.

Draw off about twenty-six or twentyseven gallons, or continue so long as the spirit will burn, by the application of a lighted paper to a small quantity of it in a saucer.

Next day, when the still is perfectly cold, let it be well cleaned out, saving the remaining ingredients for further uses, as will be after directed.

Now return the spirits drawn off yesterday into the still, and add thereto ten or twelve gallons of water. Then put in the following nine ingredients, bruised andmixed as directed. These are to remain in the liquor, in a cold state, for forty-eight hours; attention being still paid to luting and stopping close, as before.

At the end of this time, kindle the fire, and work off (slowly at first) as before, until twenty-six gallons are distilled. Mix all the different runnings together in a copper vessel, kept for this purpose only; and, as for what may come over after the twentysix gallons, it must be kept, and added to the ingredients used for the making of the next quantity of Hungary water.

The nine ingredients alluded to above, are as follows :—

Fourteen ounces of nutmegs, Four ounces of cloves, Twelve ounces of cinnamon bark, Eight ounces of pimento, and Forty ounces of cassia lignum. These are to be separately broken or bruised in an iron mortar, until they are about the size of small peas. If there be any dust, it must be sifted from them before they are used.

When the above are broken, take Forty ounces of storax, Forty ounces of gum benjamin, Forty ounces of labdanum, and Forty venellios, by tale. Break and bruise the above also, but make as little dust as possible. Put the dust from these and the foregoing, together, into a coarse muslin bag, which is to be hung in the still, so that the liquor, during distillation, may extract all its virtues.

Having drawn off, in this second distillation, just twenty-six gallons, add to it, in a copper vessel, that will hold forty gallons, six gallons of orange flower-water, and eight gallons of rose-water, which has been recently made.

Now mix together ten ounces of spirit of musk, ten ounces of spirit of ambergris, half an ounce of true oil of lavender, half an ounce of good essence of bergamot, and half an ounce of oil of rhodium.

When properly mixed, put all these into the copper vessel, and stir the whole well together. It would be better, however, if

these strong perfumes were put in before the orange-flower and rose waters.

Add to all these a quart of milk, which has stood for a night, and which has had all the cream taken clearly off:, then agitate and mix the whole well together, and stop the vessel up close, until the time when it is to be used.

Remarks.

The jar ought to have a lock-cock soldered into it, to prevent accidents. This should be placed fully two inches from the bottom, in order that the milk, and other impurities, may fall to the bottom, and not flow through into the vessels in which it is drawn off for use.

If this honey-water be made in the spring, about March or April, and if the weather be fair, it will be quite fined down in the course of a month; that is, if it be not opened or disturbed. When the perfumer finds, by drawing off a little in a glass, that the milk, &c. have fallen down to the bottom, he may draw the whole off into clean andwell-seasoned stone, or glass, bottles; or much rather into another copper jar.

This composition ought never to be drawn off in rainy or cloudy weather; for then the milk is apt to rise. In warm weather it should be kept cool; and, in winter, as warm as possible. When distilled in the winter, the jars ought to be warmed, otherwise the honey-water will not be fined for five or six months.

If the honey-water be twenty years old, so much the better.

The ingredients from the first distillation should be immediately dried in the sun, otherwise they will become mouldy. When there is a considerable quantity from three or four makings, it ought to be ground in a mill, and finely sifted. They will be found to be of great use in the making of ordinary brown wash-balls,- and, with some additions, of brown powders for the hair.

The ingredients from the second distillation are of much greater value than the above, and therefore require more care in the drying. These are of great use for the best sort of gross powders, for sweet bags, &c.; and, if made into a fine powder, may be made use of, with great success, in the best sort of brown perfumed balls.

The same powder, with fresh ingredients, makes excellent pastils, to burn; and may be further used in making spirit of benjamin. For all these uses, it is necessary to attend to the receipts which will hereafter be given./ The British Perfumer 
Source

Breaking down the recipe
Ingredients that have been described in earlier posts can be found in the ingredients list on the top of the page.

First stage
Coriander seeds An herb, with a citrusy flavor. Very common in Indian cuisine.
Marjoram An herb with a citrus and pine flavor.
Calamus Aromaticus
Yellow sandalwood Aromatic tree. A common ingredient in scents
Orange and Lemon peels The dried peels of the fruits.

There ingredients are steeped in alcohol and water before being distilled. The remains of the spices are saved and dried and the liquid is returned to the still.

Second stage
Add more water and add:

Nutmeg Spice. Dried seeds. Used in cooking, but can be poisonous in large quantities.
Clove
Cinnamon
Pimento A little tricky, perhaps- Pimento can mean a red pepper but it can also mean Allspice, and that is what it means here. That spice is the dried fruits of the of the Pimenta dioica plant
Cassia Sometimes called Bastard cinnamon. Has less taste and rougher texture than true cinnamon and is therefore cheaper.
Storax
Gum Benjamin or Benzoin resin
Labdanum
Venellios Tonka bean, a fragrant seed of the Tonka bean tree; used in perfumes and medicines and as a substitute for vanilla. EDIT: After further research, Venellios is NOT Tonka bean, but an inferior quality of Vanilla. Tonka would probably work well as a substitute, though.

Let it steep again and then distill. Once again the remains are saved and dried, but keep them separate from the first remains.

Third stage
Add

Spirit of Musk Animalistic scent originally derived from the glands from various animals, like musk deer. Today synthetic musk is almost exclusively used. Probably the most common base note in perfumes. Spirit of musk is an alcohol extract.
Spirit of Ambergris Ambergris is a waxy substance that comes from the digestive tracks of Sperm whales. Prepared it smells wonderful and has been used as fixative and base note in perfume for a long time. It can be ethically harvested, but the price is very high so usually synthetic substitutes are used. Spirit of ambergris is an alcohol extract.
Lavender oil
Bergamot essence Comes from Bergamot orange, which looks like a yellow orange. Used in scents and to flavor Earl Grey tea.
Rhodium oil, or Rosewood oil
Orange flower water A distillation of fresh bitter-orange blossoms
Rose water
Milk

Stir and leave it to settle

Fourth stage
When the milk, along with any impurities has settled at the bottom, decant the perfume into suitable bottles.
 
The dried remains can be used to perfume scent bags and powder.

My thoughts
There are a lot of ingredients in the recipe and with steeping and distilling it takes several days to come to the end of the third stage. The recipe suggests that the fourth stage will take months. The recipe also has huge quantities, which isn’t surprising as Charles Lillie was a perfumer by trade. I would really like to try this one, on a much smaller scale, of course. Most of the perfume recipes I have read demand real ambergris and musk, which would mean trying to convert it, as essence if what I can get my hand on. This recipe, as you can see, doesn’t need any such thing.

The problem that needs to be solved is the distillation process. Steam distillation in short, short is boiling water, making the steam go through the scent matter, leading the condensed liquid into another container and cool it. Hey presto, scent! I don’t really have the room to by any fancy apparatus, but I have found some simpler arrangements, like this one. For a smaller amount, it does seem to be doable.
 
I wonder if the perfume turns out spicy or flowery. The first batch of ingredients all have a citrusy scent, which ought to mean that the top notes will have a lemon quality. Then it would have spicy/resinous middle tones and muck and ambergris as base. Sounds quite a lot like a perfume I would enjoy!
Alchemy satire, 18th-century artwork